Posted by admin on Sunday, June 14, 2009 · Leave a Comment
first idea would be adding the solution to the solid-------you place the solid in some vial you can degass before adding the solvent with a cannula or a dry syringe (i prefer the cannula solution)
another way would be adding some solvent to the solid and when it dissolves adding it to the solution as described above
if your solution is not extremely sensitive it is ok to open the vial and add the solid as long as there is gas flow.
I guess a good idea might be a glove bag (there are disposable ones ~20$) which you fill with a gas (nitrogen or argon) and work freely, though i don't know how much you can trust them.
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